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Initially we also incubated suspensions of crystals with TNB for 30 minutes prior to grid preparation but this did not improve diffraction

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Thus, using the ultrasound-assisted method to prepare cyclodextrin-based metalorganic frameworks could synthesize cyclodextrin-based metalorganic framework crystals with uniform size and morphology via optimizing the ultrasound power, reaction time, and reaction temperature during the synthesis process (Shen et al